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GCSE/Chemistry/Edexcel

CC2States of matter and mixtures — separation techniques, distillation, chromatography

Notes

States of matter and mixtures

The three states of matter

StateParticle arrangementEnergyShapeVolume
SolidRegular lattice, tightly packedLowestFixedFixed
LiquidRandom, close togetherMediumNo fixed shapeFixed
GasRandom, far apart, fast-movingHighestNo fixed shapeFills container

Changes of state

Melting (solid → liquid): particles gain enough energy to overcome their fixed lattice positions. Boiling/evaporation (liquid → gas): particles break free entirely. Condensation (gas → liquid): particles lose energy, intermolecular forces pull them together. Freezing (liquid → solid): particles lose energy, return to fixed positions. Sublimation (solid → gas directly): e.g. iodine, dry ice (CO₂).

Edexcel Core Practical CP5 — Paper chromatography

Paper chromatography separates mixtures of soluble substances (e.g. food dyes, inks). Method:

  1. Draw a pencil baseline on chromatography paper (pencil is insoluble).
  2. Spot the sample onto the baseline.
  3. Stand paper in solvent (e.g. water, ethanol) below the baseline.
  4. Allow solvent to run up by capillary action.
  5. Remove and mark solvent front immediately.
  6. Calculate Rꜰ values.

Rꜰ = distance travelled by substance ÷ distance travelled by solvent front.

Rꜰ values are always between 0 and 1. A substance with low solubility in the solvent has a low Rꜰ; high solubility → high Rꜰ. Rꜰ values are fixed for a given substance in a given solvent — used for identification.

Separating mixtures

The technique chosen depends on the nature of the mixture:

Filtration

Separates an insoluble solid from a liquid. Filter paper in a funnel; the residue stays on the paper; the filtrate passes through.

Crystallisation

Separates a soluble solid from a solution. Evaporate the solvent until the solution is saturated, then allow to cool slowly. Crystals form because solubility decreases at lower temperatures.

Simple distillation

Separates a solvent from a dissolved solid (or two liquids with very different boiling points). The solution is heated; the liquid with the lower boiling point evaporates first; vapour passes through a condenser and is collected.

Fractional distillation

Separates a mixture of liquids with close boiling points (e.g. ethanol/water mixture, or crude oil fractions). A fractionating column maintains a temperature gradient; each component condenses at its own boiling point.

Edexcel exam note: choosing the method

  • Salt from salt water → evaporation / crystallisation
  • Ink colours → chromatography
  • Insoluble sand from salt water → filter (then evaporate to get salt)
  • Ethanol from ethanol/water mixture → fractional distillation

Pure substances vs mixtures

An element contains only one type of atom. A compound contains two or more elements chemically bonded. A mixture contains two or more substances NOT chemically bonded — they retain their individual properties.

A pure substance (element or compound) has a sharp melting point. A mixture melts over a range of temperatures. Edexcel Paper 1 often asks you to interpret melting point data to decide if a substance is pure.

Common mistakes

  1. Confusing filtration and centrifugation: filtration is gravity + filter paper; centrifugation spins the mixture (used in biology).
  2. Rꜰ > 1: this cannot happen. Check your measurements.
  3. Pencil vs pen on the baseline: always pencil — ink runs in the solvent.
  4. Simple vs fractional distillation: if boiling points are similar, you need fractional; if very different, simple works.

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Practice questions

Try each before peeking at the worked solution.

  1. Question 15 marks

    Chromatography — Rꜰ calculation (CP5)

    Edexcel Paper 1 — Core Practical CP5

    A student carried out paper chromatography to identify food colourings in two samples (X and Y). The solvent front moved 12.0 cm from the baseline.

    Colouring A in sample X moved 9.0 cm.
    Colouring B in sample X moved 4.8 cm.
    Colouring C in sample Y moved 9.0 cm.
    Colouring D in sample Y moved 7.2 cm.

    (a) Calculate the Rꜰ value for colouring A. (2 marks)
    (b) A student claims colouring A in sample X is the same substance as colouring C in sample Y. Is there evidence to support this claim? Give a reason. (2 marks)
    (c) Explain why the pencil line (baseline) must be drawn in pencil, not ink. (1 mark)

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  2. Question 27 marks

    Choosing a separation technique

    Edexcel Paper 1

    Describe the best technique to separate each mixture and explain why.

    (a) Rock salt (sand + salt) dissolved in water to form a solution, then you want to recover pure dry salt. (3 marks)
    (b) A mixture of ethanol (b.p. 78°C) and propanol (b.p. 97°C). (2 marks)
    (c) A coloured ink containing three different dyes. (2 marks)

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  3. Question 34 marks

    Pure substance vs mixture from melting point data

    Edexcel Paper 1

    Two samples, P and Q, are tested by measuring how their temperatures change as they are heated.

    Sample P: temperature rises steadily, then remains constant at 65°C as it melts, then rises again.
    Sample Q: temperature rises steadily; melting begins at 52°C and finishes at 68°C.

    (a) Which sample, P or Q, is a pure substance? Give a reason. (2 marks)
    (b) What does the flat section on sample P's heating curve represent? (1 mark)
    (c) Suggest a method that could be used to separate sample Q into its components. (1 mark)

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  4. Question 47 marks

    Distillation setup and explanation

    Edexcel Paper 1

    A student wants to obtain pure water from a salt solution using simple distillation.

    (a) Draw and label the apparatus for simple distillation. Include: heat source, flask, thermometer, condenser, collection vessel. (4 marks)
    (b) Explain why the thermometer bulb should be positioned at the side-arm of the flask (not submerged in liquid). (2 marks)
    (c) Why is simple distillation not suitable for separating ethanol from water? (1 mark)

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Flashcards

CC2 — States of matter and mixtures — separation techniques, distillation, chromatography

8-card SR deck for Edexcel Chemistry topic CC2

8 cards · spaced repetition (SM-2)