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C4.7The pH scale and neutralisation: H⁺ and OH⁻ ions, indicators and titrations (required practical)

Notes

pH, neutralisation and titrations

Acids and alkalis are defined by the ions they release in water:

  • Acid → releases H⁺ ions in solution.
  • Alkali → soluble base that releases OH⁻ ions in solution.

The pH scale measures how acidic or alkaline a solution is.

The pH scale

  • 0–6: acidic (lower pH = stronger acid).
  • 7: neutral (pure water).
  • 8–14: alkaline (higher pH = stronger alkali).

Universal indicator changes colour through red → orange → yellow (acidic) → green (neutral) → blue → purple (alkaline). A pH probe/meter gives a numerical value — more accurate.

Neutralisation

When acid + alkali react, the H⁺ and OH⁻ combine:

H⁺(aq) + OH⁻(aq) → H₂O(l)

This is the ionic equation for all neutralisations. The other ions (the spectator ions) form the salt:

HCl + NaOH → NaCl + H₂O

Required practical: titration of HCl with NaOH

Aim: find the exact volume of dilute HCl needed to neutralise 25.0 cm³ of NaOH solution of known concentration.

Apparatus: burette, pipette + filler, conical flask, white tile, methyl orange indicator (or phenolphthalein).

Procedure:

  1. Use a pipette to transfer 25.0 cm³ of NaOH solution into a conical flask.
  2. Add a few drops of methyl orange indicator (yellow in alkali).
  3. Fill burette with HCl, take initial reading at the meniscus.
  4. Run HCl into the flask, swirling, until the indicator just turns red (end-point).
  5. Record final burette reading. Calculate titre = final − initial.
  6. Repeat for concordant results (within 0.1 cm³). Take the mean.

The end-point is when neutralisation is complete: equal moles of H⁺ and OH⁻ have reacted.

Indicator choice

  • Methyl orange: yellow (alkaline) → red (acidic). Sharp colour change.
  • Phenolphthalein: pink (alkaline) → colourless (acidic). Sharp colour change.
  • Universal indicator gives a gradual change, so it's not used for titrations.

Worked exampleWorked example — concentration calculation (HT links to C3.7)

In a titration, 25.0 cm³ of 0.10 mol/dm³ NaOH is exactly neutralised by 20.0 cm³ of HCl. Find concentration of HCl.

  • moles NaOH = 0.025 × 0.10 = 0.0025
  • mole ratio NaOH : HCl = 1 : 1, so moles HCl = 0.0025
  • conc HCl = 0.0025 / 0.020 = 0.125 mol/dm³

Common mistakes

  • Using universal indicator — gradual colour change unsuitable for end-point.
  • Reading meniscus from wrong angle — read at eye level, bottom of meniscus.
  • Not rinsing burette with the acid before filling — dilutes it.
  • Forgetting to swirl — incomplete mixing leads to overshooting.
  • Forgetting to repeat for concordancy.

Common acids and bases (memorise)

AcidFormulaAnion
HydrochloricHClCl⁻
SulfuricH₂SO₄SO₄²⁻
NitricHNO₃NO₃⁻
BaseFormulaCation
Sodium hydroxideNaOHNa⁺
Potassium hydroxideKOHK⁺
AmmoniaNH₃ (NH₄OH in soln)NH₄⁺

Links

Builds on C4.4 (acid reactions). Sets up C4.8 (strong vs weak acids HT) and C3.7 (concentration calculations HT).

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Practice questions

Try each before peeking at the worked solution.

  1. Question 12 marks

    pH scale (F)

    (F1) State the pH of a neutral solution and the pH range of strong alkalis.

    [Foundation — 2 marks]

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  2. Question 21 mark

    Ionic equation (F)

    (F2) Write the ionic equation for any neutralisation between an acid and an alkali.

    [Foundation — 1 mark]

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  3. Question 32 marks

    Indicator choice (F)

    (F3) Why is universal indicator not suitable for titrations?

    [Foundation — 2 marks]

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  4. Question 43 marks

    Method (C)

    (F/H4) Describe how to obtain a concordant titre using burette readings.

    [Crossover — 3 marks]

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  5. Question 53 marks

    Acid concentration (H)

    (H5) 25.0 cm³ of 0.20 mol/dm³ NaOH is neutralised by 24.0 cm³ of HCl. Calculate the concentration of HCl.

    [Higher — 3 marks]

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  6. Question 62 marks

    Anomaly handling (H)

    (H6) A student gets titres of 24.10, 24.20, 24.65, 24.15 cm³. Calculate the mean titre to be used for further calculations.

    [Higher — 2 marks]

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  7. Question 72 marks

    Burette technique (H)

    (H7) Explain why the burette is rinsed with the acid before filling.

    [Higher — 2 marks]

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Flashcards

C4.7 — pH, neutralisation, titrations

10-card deck on the pH scale, ionic equations and titration technique.

10 cards · spaced repetition (SM-2)